Might mean (unverified): Relating to the testing of metals.
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We found 2 dictionaries that define the word docimastical:

General (2 matching dictionaries)
  1. docimastical: Merriam-Webster
  2. docimastical: Wiktionary

Definitions from Wiktionary (Docimastical)

adjective:  Alternative form of docimastic [(dated) of, or relating to an experiment, test or assay]

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