Might mean (unverified): Remove volatile components through heating.
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We found 2 dictionaries that define the word devolatilise:

General (2 matching dictionaries)
  1. devolatilise: Wiktionary
  2. devolatilise: Dictionary.com

Definitions from Wiktionary (Devolatilise)

verb:  Alternative form of devolatilize [(transitive) To remove volatile components from]

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